ChemInform Abstract: High‐Temperature, High‐Pressure Hydrothermal Synthesis and Characterization of a Salt‐Inclusion Mixed‐Valence Uranium(V,VI) Silicate: [Na9F2] [(UVO2)(UVIO2)2 (Si2O7)2].

Yu‐Chih Chang; Wen‐Jung Chang; S. Boudin; Kwang‐Hwa Lii

doi:10.1002/chin.201334020

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ChemInform Abstract: High‐Temperature, High‐Pressure Hydrothermal Synthesis and Characterization of a Salt‐Inclusion Mixed‐Valence Uranium(V,VI) Silicate: [Na₉F₂] [(U^VO₂)(U^VIO₂)₂ (Si₂O₇)₂].

Yu‐Chih Chang Wen‐Jung Chang S. Boudin Kwang‐Hwa Lii

Year: 2013 Journal: ChemInform Vol: 44 (34) Publisher: Wiley

DOI: 10.1002/chin.201334020

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Abstract

Abstract The title compound is hydrothermally synthesized from an aqueous mixture of UO 3 , NaOH, NaF, Na 2 HPO 4 , and Na 2 SiO 3 in a molar ratio of Na:F:U:P:Si = 39:5:1:2:10 (autoclave, 160 MPa, 585 °C, 2 d, 71% yield).

Keywords:

Chemistry Autoclave Hydrothermal circulation Silicate Aqueous solution Uranium Valence (chemistry) Nuclear chemistry Molar ratio Yield (engineering) Hydrothermal synthesis High pressure Inorganic chemistry Hydrothermal reaction Mineralogy Analytical Chemistry (journal) Physical chemistry Metallurgy Chemical engineering Organic chemistry

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Radioactive element chemistry and processing

Physical Sciences → Chemistry → Inorganic Chemistry

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ChemInform Abstract: High‐Temperature, High‐Pressure Hydrothermal Synthesis and Characterization of a Salt‐Inclusion Mixed‐Valence Uranium(V,VI) Silicate: [Na₉F₂] [(U^VO₂)(U^VIO₂)₂ (Si₂O₇)₂].

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