Syntheses with stable isotopes: Acetic‐1‐13C,‐2‐13C,‐13C2, and ‐12C2 acids

Donald G. Ott; Vernon N. Kerr

doi:10.1002/jlcr.2580120114

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Syntheses with stable isotopes: Acetic‐1‐¹³C,‐2‐¹³C,‐¹³C₂, and ‐¹²C₂ acids

Donald G. Ott Vernon N. Kerr

Year: 1976 Journal: Journal of Labelled Compounds and Radiopharmaceuticals Vol: 12 (1)Pages: 119-125 Publisher: Wiley

DOI: 10.1002/jlcr.2580120114

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Abstract

Abstract Rhodium‐catalyzed carbonylation of methanol at mild temperature and pressure has been developed for small‐ and large‐scale preparations of the carbon isotope isomers of acetic acid.

Keywords:

Chemistry Carbon-13 Acetic acid Methanol Isotope Carbonylation Kinetic isotope effect Rhodium Stable isotope ratio Carbon-14 Isotopes of carbon Radiochemistry Oxygen-18 Carbon monoxide Catalysis Deuterium Nuclear chemistry Organic chemistry Nuclear physics Physics

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Chemical Reactions and Isotopes

Life Sciences → Pharmacology, Toxicology and Pharmaceutics → Pharmaceutical Science

Mass Spectrometry Techniques and Applications

Physical Sciences → Chemistry → Spectroscopy

Analytical Chemistry and Chromatography

Physical Sciences → Chemistry → Spectroscopy

Syntheses with stable isotopes: Acetic‐1‐¹³C,‐2‐¹³C,‐¹³C₂, and ‐¹²C₂ acids

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