Abstract

The\nmagnetic susceptibility of synthesized magnetite (Fe<sub>3</sub>O<sub>4</sub>) microspheres was found to decline after the growth\nof a metal–organic framework (MOF) shell on the magnetite core.\nDetailed structural analysis of the core–shell particles using\nscanning electron microscopy, transmission electron microscopy, atom\nprobe tomography, and<sup>57</sup>Fe–Mössbauer spectroscopy\nsuggests that the distribution of MOF precursors inside the magnetic\ncore resulted in the oxidation of the iron oxide core.

Keywords:
Magnetite Transmission electron microscopy Iron oxide Oxide Shell (structure)

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