Microwave Assisted Green Synthesis of Silver Nanoparticles Using Mulberry Leaves Extract and Silver Nitrate Solution

Abstract

In this work, silver nanoparticles (AgNPs) were synthesized quickly and in an eco-friendly manner using the extract of Mulberry leaves and aqueous solution of silver nitrate without any toxic chemicals (Yuet et al. Int. J. Nanomed. 2012, 7, 4263–4267; Krishnakuma and Adavallan. Adv. Nat. Sci. Nanosci. Nanotechnol. 2014, 5, 025018). The Mulberry leaves extract functions as both a stabilizing and reducing agent. The UV-Vis spectroscopy shows a peak maximum at 430 nm. The transmission electron microscopy (TEM) image illustrated of synthesized AgNPs were nearly spherical-shaped particles whose sizes range from 15 to 20 nm. The TEM image of Nano Silver solution sample synthesized by the microwave assisted method shows nearly spherical particles, with an average particle size estimated at 10 nm. The absorption UV-vis spectrum of silver nanoparticles synthesized by the microwave assisted method (AgNPsmw) shows a sharp absorption band around 415 nm. The UV-Vis spectrum of AgNPsmw after two months of storage shows negligible peak changes of silver nanoparticles.