Crystal structure of [Pd(NH3)4]3[Ir(NO2)6]2·H2O
A. A. RybinskayaE. A. ShusharinaPavel E. PlyusninYu. V. ShubinС. В. КореневS. А. Gromilov
Abstract
A single crystal of [Pd(NH3)4]3[Ir(NO2)6]2·H2O double complex salt is studied by X-ray diffraction. Crystallographic characteristics are as follows: a = 21.0335(5) Å, b = 8.0592(2) Å, c = 21.3452(5) Å, β = 91.254(1)°, V = 3617.43(15) Å3, P21/c space group, Z = 4, d x = 2.714 g/cm3. Single-layer pseudohexagonal packing of complex anions is determined along the [−1 0 1] direction in the structure. Complex cations and crystallization water molecules are located between the mentioned layers.
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