Crystal structure of caesium tetrathioantimonate(V), Cs3SbS4

Abstract

DiscussionThis compound is isostructural to Rb3SbS4 [ 1 ].The structure consists of isolated anionic SbS4 tetrahedra surrounded by Cs cations.Table 1.Data collection and handling.Crystal: red block, size 0.16 χ 0.12 χ 0.12 mm Wavelength: Mo Ka radiation (0.71073 Â) μ• 123.20 cm" 1 Diffractometer, scan mode: Bruker AXS SMART CCD, 600 frames, Δω = 0.3°, φ = 0, 120,240 2dmu: 46.52° N(hkl)mnsinDd* N(MJ)unique: 6872,870 Criterion for /obs, N(hkl)g¿ /obs>2o-(W, 574 N(param)xefaxd: 43