JOURNAL ARTICLE

A novel synthesis of highly ordered P‐SBA‐15 mesoporous materials

Shanmugam VetrivelYun‐Chih LinChun‐Jern PanMing‐Yao ChengBing−Joe Hwang

Year: 2010 Journal:   Journal of the Chinese Institute of Engineers Vol: 33 (1)Pages: 99-103   Publisher: Taylor & Francis

Abstract

Abstract A simple synthesis method is presented to prepare highly ordered novel P‐SBA‐15 materials, which can provide additional BrØnsted acid sites for potential applications in catalysis. The developed materials have been unambiguously characterized by various techniques such as SAXS, nitrogen physisorption, SEM, TEM, 31PNMR and FT‐IR spectroscopy. The SAXS and TEM results revealed well‐ordered hexagonal arrays of mesoporous materials. 31PNMR and EDS results confirmed the incorporation of phosphorous in the SB A‐15 network. The method can provide an efficient way to synthesize high phosphorous content mesoporous silica with ordered structure.

Keywords:
Physisorption Small-angle X-ray scattering Mesoporous material Materials science Hexagonal crystal system Catalysis Mesoporous silica Chemical engineering Nanotechnology Crystallography Scattering Organic chemistry Chemistry

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3
Cited By
0.16
FWCI (Field Weighted Citation Impact)
14
Refs
0.49
Citation Normalized Percentile
Is in top 1%
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Citation History

Topics

Mesoporous Materials and Catalysis
Physical Sciences →  Materials Science →  Materials Chemistry
Chemical Synthesis and Characterization
Physical Sciences →  Environmental Science →  Industrial and Manufacturing Engineering
Polyoxometalates: Synthesis and Applications
Physical Sciences →  Materials Science →  Materials Chemistry

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