Sr3[MnN3] und Ba3[MnN3], die ersten Nitridomanganate(III): Trigonal-planare Anionen [MnIIIN3]6- / Sr3[MnN3] and Ba3[MnN3], the First Nitridomanganates(III): Trigonal-Planar Anions [MnIIIN3]6-

A. Tennstedt; Caroline Röhr; Rüdiger Kniep

doi:10.1515/znb-1993-0614

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Sr₃[MnN₃] und Ba₃[MnN₃], die ersten Nitridomanganate(III): Trigonal-planare Anionen [Mn^IIIN₃]^6- / Sr₃[MnN₃] and Ba₃[MnN₃], the First Nitridomanganates(III): Trigonal-Planar Anions [Mn^IIIN₃]^6-

A. Tennstedt Caroline Röhr Rüdiger Kniep

Year: 1993 Journal: Zeitschrift für Naturforschung B Vol: 48 (6)Pages: 794-796 Publisher: De Gruyter

DOI: 10.1515/znb-1993-0614

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Abstract

Sr 3 [MnN 3 ] (hexag. P6 3 /m (Nr. 176); a = 764.2(1) pm, c = 529.8(1) pm; Z = 2) and Ba 3 [MnN 3 ] (hexag. P6 3 /m (Nr. 176); a = 805.0(2) pm, c = 558.6(1) pm; Z = 2) are isotypes of the Ba 3 [FeN 3 ] crystal structure and contain trigonal-planar anions [MnN 3 ] 6- with D 3h -symmetry (Mn—N: 174.1(13) pm/173.7(12) pm). The compounds were prepared by reaction of mixtures of Li, Sr/Ba and Mn (molar ratio 2:1:1) in tungsten crucibles with nitrogen (1 atm) at 850°C.

Keywords:

Trigonal crystal system Tungsten Crystallography Chemistry Manganese Crystal structure Analytical Chemistry (journal) Nitrogen Molar ratio Mineralogy

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Sr₃[MnN₃] und Ba₃[MnN₃], die ersten Nitridomanganate(III): Trigonal-planare Anionen [Mn^IIIN₃]^6- / Sr₃[MnN₃] and Ba₃[MnN₃], the First Nitridomanganates(III): Trigonal-Planar Anions [Mn^IIIN₃]^6-

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