New route for preparation and characterization of magnetite nanoparticles

Abstract

We report here the synthesis of naked magnetic nanoparticles by using a facile method. Magnetic nanoparticles were prepared by mixing and stirring two equivalents of iron(II) chloride tetrahydrate with three equivalents of iron(III) chloride hexahydrate at room temperature. The mixture was treated by adding 100 ml of 28% ammonium hydroxide. Immediately, the color of the solution turned from orange to black. The magnetite nanoparticles that precipitated were washed three times with 5% NH4OH solution using the magnetic decantation method. 2Fe(II)+3Fe(III)→NH4OHpH=9Fe3O4↓ The nanoparticles underwent full characterization. Their surface show a bunch of hydroxyl groups which can be used for further complexion and removal of many hazardous compounds.