Crystal structure of bis(triethylenetetramine) tris(zirconium) hexa(nitrilotriacetate) tetrahydrate, (NH3(CH2)2NH(CH2)2NH2(CH2)2NH3)2(Zr)3(N(CH2COO)3)6 · 4H2O

E. Haussiihl; S. Haussühl; J. Schreuer

doi:10.1515/ncrs-2000-0151

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Crystal structure of bis(triethylenetetramine) tris(zirconium) hexa(nitrilotriacetate) tetrahydrate, (NH3(CH2)2NH(CH2)2NH2(CH2)2NH3)2(Zr)3(N(CH2COO)3)6 · 4H2O

E. Haussiihl S. Haussühl J. Schreuer

Year: 2000 Journal: Zeitschrift für Kristallographie - New Crystal Structures Vol: 215 (1)Pages: 98-100 Publisher: De Gruyter

DOI: 10.1515/ncrs-2000-0151

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Abstract

C48H86Ni404oZr3, monoclinic, C12/cl (No. 15), a = 39.146(8)k,b = 9.445(2) А, с = 21.076(4)Ä, β = 116.41(3)°,V= 6979.4Ä 3 , Z = 4, p m = 1.685(2) g-спГ 3 , R gt (F) = 0.027, wR(F 2 ) = 0.073, 7= 293 K. Source of materialThe raw material was obtained by fractional crystallization of the reaction product of trietylenetetramine, nitrilotriacetic acid and ZrCU in a stoiciometric ratio at 300 K.

Keywords:

Triethylenetetramine Tetrahydrate HEXA Crystal structure Tris Zirconium Chemistry Crystallography Hydrate Carboxylate Stereochemistry Inorganic chemistry Organic chemistry

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Crystal structure of bis(triethylenetetramine) tris(zirconium) hexa(nitrilotriacetate) tetrahydrate, (NH3(CH2)2NH(CH2)2NH2(CH2)2NH3)2(Zr)3(N(CH2COO)3)6 · 4H2O

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